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Teledyne API – T101 Operation Manual EPA Protocol Calibration
189
Table 7-2. Activity Matrix for Calibration Procedure
EQUIPMENT/
SUPPLIES
ACCEPTANCE LIMITS
FREQUENCY AND METHOD OF
MEASUREMENT
ACTION IF REQUIREMENTS ARE
NOT MET
Calibration
Gases
NIST traceable Assayed against an NIST-SRM
semi-annually, Sec. 2.0.7,
(Q.A. Handbook)
Working gas standard is unstable,
and/or measurement method is
out of control; take corrective
action such as obtaining new
calibration gas.
Dilution Gas Zero air, free of
contaminants
See Section 2.9.2 (Q.A.
Manual)
Return to supplier or take
appropriate action with
generation system
Multi-Point
Calibration
Use calibration
procedure in Section
2.2 (Q.A. Handbook);
also Federal Register
Perform at least once every
quarter or anytime a level span
check indicates a discrepancy,
or after maintenance which
may affect the calibration;
Section 2.5 (Q.A. Manual)
Repeat the calibration
7.1.2. DATA RECORDING DEVICE
Either a strip chart recorder, data acquisition system, digital data acquisition system
should be used to record the data from the Mode; T101 RS-232 port or analog outputs. If
analog readings are being used, the response of that system should be checked against a
NIST referenced voltage source or meter. Data recording device should be capable of bi-
polar operation so that negative readings can be recorded.
7.1.3. RECOMMENDED STANDARDS FOR ESTABLISHING
TRACEABILITY
To assure data of desired quality, two considerations are essential: (1) the measurement
process must be in statistical control at the time of the measurement and (2) the
systematic errors, when combined with the random variation in the measurement process,
must result in a suitably small uncertainty.
Evidence of good quality data includes documentation of the quality control checks and
the independent audits of the measurement process by recording data on specific forms or
on a quality control chart and by using materials, instruments, and measurement
procedures that can be traced to appropriate standards of reference. To establish
traceability, data must be obtained routinely by repeat measurements of standard
reference samples (primary, secondary, and/or working standards). More specifically,
working calibration standards must be traceable to standards of higher accuracy, such as
those listed in Table 7-1.
Cylinders of working gas traceable to NIST-SRM's (called EPA Protocol Calibration
Gas) are also commercially available (from sources such as Scott Specialty Gases, etc.).
7.1.4. EPA CALIBRATION USING PERMEATION TUBES
Teledyne API does not recommend the use of permeation tubes as a source of span gas
for EPA protocol calibration operations.
07266B DCN6485
- MODEL T101 1
- UV FLUORESCENCE H 1
- S ANALYZER 1
- SAFETY MESSAGES 5
- CONSIGNES DE SÉCURITÉ 6
- WARRANTY 7
- ABOUT THIS MANUAL 9
- REVISION HISTORY 9
- 07266B DCN6485 10
- TABLE OF CONTENTS 11
- LIST OF APPENDICES 16
- LIST OF FIGURES 17
- LIST OF TABLES 18
- 1. INTRODUCTION 21
- 1.2. OPTIONS 22
- PARAMETER 25
- DESCRIPTION 25
- 2.2.1. SAFETY 26
- 2.2.2. EMC 26
- 3. GETTING STARTED 27
- 3.2. INSTRUMENT LAYOUT 28
- 3.2.2. REAR PANEL 32
- 3.3. ELECTRICAL CONNECTIONS 35
- ANALOG OUT 36
- 3.4. PNEUMATIC CONNECTIONS 41
- FL O W 44
- CO NTR O L 44
- Permeation Tube Heater 50
- INSTRUMENT CHASSIS 51
- VACUUM MANIFOLD 51
- 51
- NO 51
- CALIBRATION 52
- 3.5.4. FUNCTIONAL CHECK 54
- 3.6. INITIAL CALIBRATION 55
- 3.6.2. INTERFERENCES FOR H 58
- S MEASUREMENTS 58
- 4. OPERATING INSTRUCTIONS 59
- 4.2. SAMPLE MODE 60
- 4.2.2. WARNING MESSAGES 63
- 4.3. CALIBRATION MODE 64
- 4.4. SETUP MODE 66
- 4.4.4.7. Range Units 74
- 4.4.4.8. Dilution Ratio 75
- Table 4-6. Password Levels 76
- PRIMARY SETUP MENU 77
- SECONDARY SETUP MENU 78
- NO. VARIABLE DESCRIPTION 80
- ALLOWED 80
- See Section 6.8.1 81
- Press the PREV 82
- FUNCTIONS 83
- 4.6.1. SIGNAL I/O 85
- Table 4-12 88
- 4.6.3), then press: 93
- (Figure 4-5) 95
- 4.6.3.6. AIN Calibration 97
- 4.6.4. OPTIC TEST 99
- 4.6.5. ELECTRICAL TEST 100
- 4.6.6. LAMP CALIBRATION 101
- 4.6.7. PRESSURE CALIBRATION 102
- 4.6.8. FLOW CALIBRATION 103
- 4.6.9. TEST CHANNEL OUTPUT 104
- COMMUNICATION PORTS 105
- 4.7.4. RS-485 CONFIGURATION 109
- Contact your IT 113
- Network Administrator 113
- BUTTON FUNCTION 115
- >\ 115
- 4.7.7. USB CONFIGURATION 116
- RS-232 port 120
- 4.7.9. MODBUS SET UP 121
- ID DESCRIPTION 123
- 4.7.11. COM PORT BAUD RATE 125
- 4.7.12. COM PORT TESTING 126
- 4.8.1. DAS STRUCTURE 127
- 4.8.1.2. DAS Parameters 128
- 4.8.2. DEFAULT DAS CHANNELS 130
- LIST OF PARAMETERS 131
- LIST OF CHANNELS 131
- 0) CONC: ATIMER, 4, 800 133
- 4.8.2.3. Trigger Events 135
- Press SET> until… 136
- 4.8.2.6. Number of Records 139
- 4.8.2.8. Compact Report 141
- 4.8.2.9. Starting Date 141
- 4.8.2.11. HOLDOFF Feature 143
- 5. REMOTE OPERATION 145
- 5.1.1.2. Control Inputs 147
- 5.1.2.3. Command Syntax 150
- 5.1.2.4. Data Types 150
- 5.1.2.5. Status Reporting 151
- Parameter Standard Hessen 157
- Data Bits 8 7 157
- Stop Bits 1 2 157
- Parity None Even 157
- Duplex Full Half 157
- 6. CALIBRATION PROCEDURES 165
- 6.1.2. ZERO AIR 166
- 6.1.3. GAS STANDARDS 166
- 6.1.4. PERMEATION TUBES 166
- 6.2. MANUAL CALIBRATION 167
- Chassis 168
- STEP TWO: Set the expected H 169
- (At high 172
- span gas value: 173
- ZERO/SPAN VALVES 176
- No Valve Options Installed 180
- Table 6-2. AutoCal Modes 181
- 0.5 hours later each day 183
- Default 184
- REPORTING RANGE MODES 185
- MEASUREMENT MODE 186
- 6.10. CALIBRATION QUALITY 187
- 7. EPA PROTOCOL CALIBRATION 189
- TRACEABILITY 191
- 7.1.5. CALIBRATION FREQUENCY 192
- 7.1.6. RECORD KEEPING 192
- Table 7-3. Activity Matrix 193
- 7.3. ZERO AND SPAN CHECKS 195
- 7.4.1. PRECISION CALIBRATION 196
- 7.4.2. PRECISION CHECK 196
- 7.7. REFERENCES 198
- 8. INSTRUMENT MAINTENANCE 199
- 198 047400102 Rev XC 200
- 8.3. MAINTENANCE PROCEDURES 204
- 8.3.3. MAINTAINING THE SO 205
- SCRUBBER 205
- To check to see if your SO 206
- 8.3.5. MAINTAINING THE H 208
- CONVERTER 208
- 8.3.5.3. Changing the H 209
- 9.1. GENERAL TROUBLESHOOTING 213
- 9.1.4. STATUS LEDS 220
- Motherboard 221
- CPU Status LED 221
- 9.2. GAS FLOW PROBLEMS 222
- 9.3. CALIBRATION PROBLEMS 223
- 9.3.2. NO RESPONSE 224
- 9.3.6. NON-LINEAR RESPONSE 225
- 9.4.1. EXCESSIVE NOISE 226
- 9.4.2. SLOW RESPONSE 226
- 9.5. SUBSYSTEM CHECKOUT 227
- 9.5.4. DC POWER SUPPLY 229
- 9.5.8. RELAY BOARD 230
- 9.5.5. I 230
- 9.5.6. TOUCHSCREEN INTERFACE 230
- 9.5.7. LCD DISPLAY MODULE 230
- 9.5.9. MOTHERBOARD 231
- 9.5.10. CPU 232
- 9.5.11. RS-232 COMMUNICATION 233
- 9.5.12. PMT SENSOR 234
- 9.5.17. IZS OPTION 235
- 9.6. REPAIR PROCEDURES 236
- 9.6.3. REPLACING THE UV LAMP 239
- 9.8. TECHNICAL ASSISTANCE 243
- 10. PRINCIPLES OF OPERATION 245
- SO2OH2O3SH2 246
- SOaxexp1IIa 247
- = The rate at which the SO 248
- = Amount of excited state SO 248
- 10.2.1. UV SOURCE LAMP 249
- 10.2.3. THE PMT 250
- 10.2.4. OPTICAL FILTERS 251
- 10.2.5. OPTICAL LENSES 252
- 10.2.6.3. Dilution 254
- 10.2.6.5. Light Pollution 254
- 10.3. PNEUMATIC OPERATION 255
- 10.3.1. SAMPLE GAS FLOW 256
- SWITCHING 257
- 10.3.3. FLOW RATE CONTROL 257
- 10.3.6. SO 259
- 10.3.7. PNEUMATIC SENSORS 260
- CPU Card 261
- 10.4.1. CPU 263
- Figure 10-13. PMT Assembly 265
- 10.4.5. PMT COOLING SYSTEM 266
- 10.4.6. PMT PREAMPLIFIER 267
- PMT Preamp PCA 268
- 10.4.8.1. Heater Control 269
- 10.4.8.2. Valve Control 269
- 10.4.10.1. A to D Conversion 271
- 10.4.10.2. Sensor Inputs 271
- 10.4.11. ANALOG OUTPUTS 272
- 10.4.13. I 273
- C DATA BUS 273
- 10.4.14. POWER UP CIRCUIT 273
- 10.7.1. ADAPTIVE FILTER 276
- FEATURE 278
- 11.4.1. GENERAL RULES 282
- AND MAINTENANCE 284
- DO NOT use pink-poly bags 286
- GLOSSARY 287
- (Primary Setup Menu) 294
- ENTER SETUP PASS: 818 297
- GAS TYPE 299
- REPORTED 299
- Name Description 320
- Name Description Units 322
- MODBUS Coil Registers 326
- (single-bit; read/write) 326
- T101 Spare Parts List 329
- 07266B DCN6845 332
- Appendix C 333
- T101, M101E 333
- Auxiliary I/O Board (USB) 356
- Auxiliary I/O Board (ADC) 357
- GUI Interface 358
- Mode R32 R45 360
- Default A A 360
- MBUS B B 360
- From ICOP CPU 371
- To LCD Display 371
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